1999 •
Efficient synthesis of N-alkylformimidoyl cyanides
Authors: PEROSA, Alvise, SELVA, Maurizio, TUNDO, Pietro
Venue: Tetrahedron Letters
Type: Publication
Abstract: N-Alkylformimidoyl cyanides (RRCHNCHCN, 1) were obtained through a very efficient oxidation of N-alkylaminoacetonitriles (RRCHNHCH2CN, 2) by aq. NaOCl. The reaction was run under very mild and simple conditions and afforded products (as EZ isomer mixtures; EZ ratio of 70–99%) in short reaction times (30–180 min), and in good to excellent yields (67–97%).
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