Authors:
Mentesana, Roberta Bruna, Buxeda I Garrigós, Jaume, Madrid I Fernández, Marisol
Abstract:
Chemical characterization was conducted by means of wavelength Dispersive X-ray fluorescence (WDXRF) analysis. The concentrations were quantified using an AxiosmAX-Advanced PANalytical spectrometer with a Rh excitation source calibrated by a suite of 56 international Geological Standards. Interferences were considered and the correction of matrix effects was done using PANanalytical Pro-Trace software for trace elements. The determined elements were: Na2O, MgO, Al2O3, SiO2, P2O5, K2O, CaO, TiO2, V, Cr, MnO, Fe2O3 (as total Fe), Co, Ni, Cu, Zn, (...)
Chemical characterization was conducted by means of wavelength Dispersive X-ray fluorescence (WDXRF) analysis. The concentrations were quantified using an AxiosmAX-Advanced PANalytical spectrometer with a Rh excitation source calibrated by a suite of 56 international Geological Standards. Interferences were considered and the correction of matrix effects was done using PANanalytical Pro-Trace software for trace elements. The determined elements were: Na2O, MgO, Al2O3, SiO2, P2O5, K2O, CaO, TiO2, V, Cr, MnO, Fe2O3 (as total Fe), Co, Ni, Cu, Zn, Ga, Rb, Sr, Y, Zr, Nb, Mo, Sn, Ba, Ce, W, Pb and Th. Minor and major elements are expressed as concentrations of oxides in percentage by mass (wt %). Trace elements are conveyed as concentrations of elements in μg g-1. Samples are prepared according to a procedure explained in Madrid i Fernández, Marisol, and Alejandro G. Sinner. "Analysing technical choices: improving the archaeological classification of Late Republican Black Gloss pottery in north-eastern Hispania consumption centres." Archaeological and Anthropological Sciences 11, no. 7 (2019): 3155-3186.
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